Chemistry 8160, Fall Semester 2009
|Week of August 24||
M: "Electromagnetic radiation interacts with matter"
W: Assignment #1: FSK 4/e Problems #1-10
F: IR Spectroscopy
|Week of August 31||W: Assignment #2: FSK 4/e Problems #11-20|
|Week of September 7||
M: No Meeting,
W: Assignment #3: FSK 4/e Problems #31-40
W: Rotational Finestructure. F: Raman Spectroscopy
|Week of September 14||
M: Raman Spectroscopy
W: Assignment: Work old tests; works exam#1 FS07 and exam#1 FS08.
|Week of September 21||
W: Assignment #4: FSK 4/e Problems 58-64 (only 7 problems this time)
All week on basics of the NMR experiment: spin, magn. moment, Zeeman effect, magnetization, effects of RF absorption, FID.
|Week of September 28||
M: delta, sigma-dia, sigma-para, and anisotropic effects (alkynes, benzene)
W: delta prediction; F: spin-spin coupling mechanism
W: Assignment #5: Chem. Shift Pred. using Pretsch, based on FSK 4/e (60, 70-73 & 77)
|Week of October 5||
All week on CNMR: Abundance (no 13C-13C coupling), 13C-H decoupling, NOE for 13C-H,
(2nI+1) rule, CNMR increment systems, CNMR of solvents
F: Assignment #6: Chem. Shift Pred. using Pretsch, based on FSK 4/e (84, 88, 89 & 95)
|Week of October 12||
M: Assignment: Work old tests (handout 10/9).
NMR all week: Solvents, NOE & T1, 13C-coupling to F, P, etc.
|Week of October 19||
HNMR all week: Spin-Spin Coupling, Chapter 5
W: Assignment #7: Multiplet Analysis, FSK 4/e (315 - 324)
F: Computer Lab: NMR Spectrum Simulation
|Week of October 26||
M: Chapter 5 wrap-up. W: Start Chapter 6.
W: Assignment #8: Reading on Intramolecular Proton Transfer
|Week of November 2||M: NMR (Chiral) Shift Reagents.
W, F: MO Theory of UV/Vis spectroscopy (Chapter 7)
F: Assignment #9: UV/Vis Focus Module, FSK 4/e (101, 103-105, 110)
|Week of November 9||
M: DA-Substitution, UV/Vis Increment Systems
W: Franck-Condon Factor. Assignment: Prepare for T#3
|Week of November 16||M: Luminescence: Fluorescence & Phosphorescence
W: Assignment #10: Focus on 2D-NMR, FSK 4/e (292 - 301)
F: Chapter 8: Ionization Methods (EI, CI, FAB, LDI, MALDI)
|Week of November 23||THANKSGIVING BREAK|
|Week of November 30||W: Assignment #11: Focus on 2D-NMR, FSK 4/e (305 - 309)|
|Week of December 7||
W: Last Lecture, Assignment: Work old tests.
M, 12/14, 9 - 11 am: Final